8.d) Zavoral Air Monitoring LabResults•
GALSON
LABORATORIES
Mr. Dave Gutterud
Indoor Environment Group
2487 7th Ave. E
North St. Paul, MN 55109
DOH ELAP# 11626
AIHA # 100324
Dear Mr. Gutterud:
Account# 23406
Login# L307847
December 31, 2013
Enclosed are the analytical results for the samples received by our laboratory on December 20, 2013. All
test results meet the quality control requirements of AIHA and NELAC unless otherwise stated in this report.
All samples on the chain of custody were received in good condition unless otherwise noted.
Results in this report are based on the sampling data provided by the client and refer only to the samples
as they were received at the laboratory. Unless otherwise requested, all samples will be discarded 14 days
from the date of this report, with the exception of IOMs, which will be cleaned and disposed of after
seven calendar days.
Current Scopes of Accreditation can be viewed at www. galsonlabs. com in the accreditations section under
the "about Galson" tab.
Please contact Patty Gregorich at (888)-432-5227, if you would like any additional information regarding
this report.
Thank you for using Galson Laboratories.
Sincerely,
Galson Laboratories
U
Mary G. Unangst
Laboratory Director
Enclosure(s)
Page 1 of 8 Report Reference:1 Generated:31-DEC-13 16:04
•
GALSON
LABORATORIES
6601 Kirkville Road
East Syracuse, NY 13057
(315) 432-5227
FAX: (315) 437-0571
www.galsonlabs.com
Client
Site
Project No.
Date Sampled
Date Received
Date Analyzed
Report ID
Diesel Particulate Matter as Carbon
Air Vol
Sample ID Lab ID liter
DP1-01 L307847-6 871.2
DP2-01 L307847-7 861.3
DP3-01 L307847-8 847.4
DP4-01 L307847-9 859.3
LABORATORY ANALYSIS REPORT
Indoor Environment Group
Scandia
4055-002
17 -DEC -13 Account No.: 23406
20 -DEC -13 Login No. L307847
27 -DEC -13
813160
COMMENTS: Please see attached lab footnote report for any applicable footnotes.
Level of quantitation: 3ug OC & EC; 5ug TC Submitted by: JAR
Analytical Method mod. NIOSH 5040; TOA Approved by : JGC
OSHA PEL NA Date : 31 -DEC -13 NYS DOH # : 11626
Collection Media 37mm QtzFt QC by: Tony D'Amico
< -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms
> -Greater Than ug -Micrograms 1 -Liters NS -Not Specified
NA -Not Applicable ND -Not Detected ppm -Parts per Million
Page 2 of 8 Report Reference:1 Generated:31-DEC-13 16:04
Total
Conc
Analyte
ug
ug/m3
Organic Carbon
15
18
Elemental Carbon
<3
<3
Total Carbon
15
18
Organic Carbon
15
17
Elemental Carbon
<3
<3
Total Carbon
15
17
Organic Carbon
12
14
Elemental Carbon
<3
<3
Total Carbon
12
14
Organic Carbon
14
16
Elemental Carbon
<3
<3
Total Carbon
14
16
COMMENTS: Please see attached lab footnote report for any applicable footnotes.
Level of quantitation: 3ug OC & EC; 5ug TC Submitted by: JAR
Analytical Method mod. NIOSH 5040; TOA Approved by : JGC
OSHA PEL NA Date : 31 -DEC -13 NYS DOH # : 11626
Collection Media 37mm QtzFt QC by: Tony D'Amico
< -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms
> -Greater Than ug -Micrograms 1 -Liters NS -Not Specified
NA -Not Applicable ND -Not Detected ppm -Parts per Million
Page 2 of 8 Report Reference:1 Generated:31-DEC-13 16:04
•
GALSON
LABORATORIES
6601 Kirkville Road
East Syracuse, NY 13057
(315) 432-5227
FAX: (315) 437-0571
www.galsonlabs.com
Client
Site
Project No.
Date Sampled
Date Received
Date Analyzed
Report ID
LABORATORY ANALYSIS REPORT
Indoor Environment Group
Scandia
4055-002
17 -DEC -13 Account No.: 23406
20 -DEC -13 Login No. L307847
27 -DEC -13
813160
Diesel Particulate Matter as Carbon
Air Vol Total Conc
Sample ID Lab ID liter Analyte ug ug/m3
DP5-01 L307847-10 847.4 Organic Carbon 13 15
Elemental Carbon <3 <3
Total Carbon 13 15
COMMENTS: Please see attached lab footnote report for any applicable footnotes.
Level of quantitation: 3ug OC & EC; 5ug TC
Analytical Method mod. NIOSH 5040; TOA
OSHA PEL NA
Collection Media 37mm QtzFt
Submitted by: JAR
Approved by : JGC
Date : 31 -DEC -13 NYS DOH # : 11626
QC by: Tony D'Amico
-Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms
> -Greater Than ug -Micrograms 1 -Liters NS -Not Specified
NA -Not Applicable ND -Not Detected ppm -Parts per Million
Page 3 of 8 Report Reference:1 Generated:31-DEC-13 16:04
•
GALSON
LABORATORIES
6601 Kirkville Road
East Syracuse, NY 13057
(315) 432-5227
FAX: (315) 437-0571
www.galsonlabs.com
Nitrogen Dioxide
Client
Site
Project No.
Date Sampled
Date Received
Date Analyzed
Report ID
LABORATORY ANALYSIS REPORT
Indoor Environment Group
Scandia
4055-002
17 -DEC -13 Account No.: 23406
20 -DEC -13 Login No. L307847
23 -DEC -13
812689
COMMENTS: Please see attached lab footnote report for any applicable footnotes.
PPM
<0.03
<0.03
<0.03
<0.03
Level of quantitation: 0.5 ug Submitted by: tmk
Analytical Method In-house: IC -SOP -14; IC Approved by : dnf
OSHA PEL 5 ppm CEIL Date : 31 -DEC -13 NYS DOH # : 11626
Collection Media 500-200 QC by: Tony D'Amico
< -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms
> -Greater Than ug -Micrograms 1 -Liters NS -Not Specified
NA -Not Applicable ND -Not Detected ppm -Parts per Million
Page 4 of 8 Report Reference:1 Generated:31 -DEC-1 3 16:04
Time
Total
Conc
Sample ID
Lab ID
minutes
ucr
ma/m3
N01-01
L307847-11
444
<0.5
<0.06
NO2-01
L307847-12
437
<0.5
<0.06
N04-01
L307847-13
428
<0.5
<0.07
N05-01
L307847-14
427
<0.5
<0.07
COMMENTS: Please see attached lab footnote report for any applicable footnotes.
PPM
<0.03
<0.03
<0.03
<0.03
Level of quantitation: 0.5 ug Submitted by: tmk
Analytical Method In-house: IC -SOP -14; IC Approved by : dnf
OSHA PEL 5 ppm CEIL Date : 31 -DEC -13 NYS DOH # : 11626
Collection Media 500-200 QC by: Tony D'Amico
< -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms
> -Greater Than ug -Micrograms 1 -Liters NS -Not Specified
NA -Not Applicable ND -Not Detected ppm -Parts per Million
Page 4 of 8 Report Reference:1 Generated:31 -DEC-1 3 16:04
•
GALSON
LABORATORIES
6601 Kirkville Road
East Syracuse, NY 13057
(315) 432-5227
FAX: (315) 437-0571
www.galsonlabs.com
Client
Site
Project No.
Date Sampled
Date Received
Date Analyzed
Report ID
LABORATORY ANALYSIS REPORT
Indoor Environment Group
Scandia
4055-002
17 -DEC -13 Account No.: 23406
20 -DEC -13 Login No. L307847
23 -DEC -13 - 27 -DEC -13
812461
Respirable Dust and Crystalline Silica: Quartz
Dust
P E L
mg % m m3 m m3
<0.050 <0.047 5.0
<0.010 ND <0.0093
<0.050 <0.047 5.0
<0.010 ND <0.0094
<0.050 <0.048 5.0
<0.010 ND <0.0096
<0.050 <0.047 5.0
<0.010 ND <0.0095
<0.050 <0.048 5.0
<0.010 ND <0.0097
COMMENTS: Please see attached lab footnote report for any applicable footnotes.
Level of quantitation:
Dust
0.050mg Q:0.010mg
Submitted by: MNS/AJD/LCC
Analytical Method
Air Vol
Sample
ID
Lab ID
Analyte
1
RD1-01
Collection Media
L307847-1
PW
Dust
1074.06
Quartz
1074.06
RD2-01
L307847-2
Dust
1061.91
Quartz
1061.91
RD3-01
L307847-3
Dust
1040.04
Quartz
1040.04
RD4-01
L307847-4
Dust
1054.62
Quartz
1054.62
RD5-01
L307847-5
Dust
1032.75
Quartz
1032.75
Dust
P E L
mg % m m3 m m3
<0.050 <0.047 5.0
<0.010 ND <0.0093
<0.050 <0.047 5.0
<0.010 ND <0.0094
<0.050 <0.048 5.0
<0.010 ND <0.0096
<0.050 <0.047 5.0
<0.010 ND <0.0095
<0.050 <0.048 5.0
<0.010 ND <0.0097
COMMENTS: Please see attached lab footnote report for any applicable footnotes.
Level of quantitation:
Dust
0.050mg Q:0.010mg
Submitted by: MNS/AJD/LCC
Analytical Method
mod.
NIOSH 0600/7500/mod.
OSHA ID -142; Gr Approved by : KRK
OSHA PEL
see
1910.1000 (Table Z-3)
Date : 30 -DEC -13 NYS DOH # : 11626
Collection Media
PVC
PW
QC by: Tony D'Amico
< -Less Than mg -Milligrams
> -Greater Than ug -Micrograms
NA -Not Applicable ND -Not Detected
mppcf -Million Particles per Cubic Foot
m3 -Cubic Meters kg -Kilograms
1 -Liters NS -Not Specified
ppm -Parts per Million
Page 5 of 8 Report Reference:1 Generated:31-DEC-13 16:04
•
GALSON
LABORATORIES
6601 Kirkville Road
East Syracuse, NY 13057
(315) 432-5227
FAX: (315) 437-0571
www.galsonlabs.com
LABORATORY FOOTNOTE REPORT
Client Name Indoor Environment Group
Site Scandia
Project No. 4055-002
Date Sampled : 17 -DEC -13 Account No.: 2340.6
Date Received: 20 -DEC -13 Login No. : L307847
Date Analyzed: 23 -DEC -13 - 27 -DEC -13
Unless otherwise noted below, all quality control results associated with the samples
were within established control limits or did not impact reported results.
Unrounded results are carried through the calculations that yield the final result and the final
result is rounded to the number of significant figures appropriate to the accuracy of the
analytical method. Please note that results appearing in the columns preceeding the final
result column may have been rounded in order to fitthe report format and therefore, if carried
through the calculations, may not yield an identical final result to the one reported.
The stated LOQs for each analyte represent the demonstrated LOQ concentrations prior to correction
for desorption efficiency (if applicable).
Unless otherwise noted below, reported results have not been blank corrected for any field blank or method blank.
L307847 (Report ID: 813160):
SOPS: ic-n5040(16)
Accuracy and mean recovery data presented below is based on a 95% confidence interval (k=2).
The estimated uncertainty applies to the media, technology, and SOP referenced in this report
and does not account for the uncertainty associated with the sampling process.
Parameter Accuracy Mean Recove
Diesel Particulate Matter as Carbon +/-7.1% 102%
L307847 (Report ID: 812689):
SOPS: IC -SOP -14(6)
Total ug corrected for a desorption efficiency of 102%.
Accuracy and mean recovery data presented below is based on a 95% confidence interval (k=2).
The estimated uncertainty applies. to the media, technology, and SOP referenced in this report
and does not account for the uncertainty associated with the sampling process.
Parameter Accuracy Mean Recovery
Nitrogen Dioxide
+/-16.7 100%
L307847 (Report ID: 812461):
Dust analytical accuracy is within +/- 0.010 mg (95% confidence interval or k=2). The estimated
uncertainty applies to the media, technology, and SOP(s) referenced in this report and does not
account for any uncertainty associated with the sampling process.
SOPS: GRAV-SOP-5(5), GRAV-SOP-6(4), ix-calibrate(8), ix-xrdashprep(19), ix-xrdreview(9), ix-xrdstdprep(20)
Accuracy and mean recovery data presented below is based on a 95% confidence interval (k=2).
The estimated uncertainty applies to the media, technology, and SOP referenced in this report
and does not account for the uncertainty associated with the sampling process.
Parameter Accuracy Mean Recovery
Quartz
+/-13.4% 95.1%
< -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms
> -Greater Than ug -Micrograms 1 -Liters NS -Not Specified
NA -Not Applicable ND -Not Detected ppm -Parts per Million
Page 6 of 8 Report Reference:1 Generated:31-DEC-13 16:04
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