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8.d) Zavoral Air Monitoring LabResults• GALSON LABORATORIES Mr. Dave Gutterud Indoor Environment Group 2487 7th Ave. E North St. Paul, MN 55109 DOH ELAP# 11626 AIHA # 100324 Dear Mr. Gutterud: Account# 23406 Login# L307847 December 31, 2013 Enclosed are the analytical results for the samples received by our laboratory on December 20, 2013. All test results meet the quality control requirements of AIHA and NELAC unless otherwise stated in this report. All samples on the chain of custody were received in good condition unless otherwise noted. Results in this report are based on the sampling data provided by the client and refer only to the samples as they were received at the laboratory. Unless otherwise requested, all samples will be discarded 14 days from the date of this report, with the exception of IOMs, which will be cleaned and disposed of after seven calendar days. Current Scopes of Accreditation can be viewed at www. galsonlabs. com in the accreditations section under the "about Galson" tab. Please contact Patty Gregorich at (888)-432-5227, if you would like any additional information regarding this report. Thank you for using Galson Laboratories. Sincerely, Galson Laboratories U Mary G. Unangst Laboratory Director Enclosure(s) Page 1 of 8 Report Reference:1 Generated:31-DEC-13 16:04 • GALSON LABORATORIES 6601 Kirkville Road East Syracuse, NY 13057 (315) 432-5227 FAX: (315) 437-0571 www.galsonlabs.com Client Site Project No. Date Sampled Date Received Date Analyzed Report ID Diesel Particulate Matter as Carbon Air Vol Sample ID Lab ID liter DP1-01 L307847-6 871.2 DP2-01 L307847-7 861.3 DP3-01 L307847-8 847.4 DP4-01 L307847-9 859.3 LABORATORY ANALYSIS REPORT Indoor Environment Group Scandia 4055-002 17 -DEC -13 Account No.: 23406 20 -DEC -13 Login No. L307847 27 -DEC -13 813160 COMMENTS: Please see attached lab footnote report for any applicable footnotes. Level of quantitation: 3ug OC & EC; 5ug TC Submitted by: JAR Analytical Method mod. NIOSH 5040; TOA Approved by : JGC OSHA PEL NA Date : 31 -DEC -13 NYS DOH # : 11626 Collection Media 37mm QtzFt QC by: Tony D'Amico < -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms > -Greater Than ug -Micrograms 1 -Liters NS -Not Specified NA -Not Applicable ND -Not Detected ppm -Parts per Million Page 2 of 8 Report Reference:1 Generated:31-DEC-13 16:04 Total Conc Analyte ug ug/m3 Organic Carbon 15 18 Elemental Carbon <3 <3 Total Carbon 15 18 Organic Carbon 15 17 Elemental Carbon <3 <3 Total Carbon 15 17 Organic Carbon 12 14 Elemental Carbon <3 <3 Total Carbon 12 14 Organic Carbon 14 16 Elemental Carbon <3 <3 Total Carbon 14 16 COMMENTS: Please see attached lab footnote report for any applicable footnotes. Level of quantitation: 3ug OC & EC; 5ug TC Submitted by: JAR Analytical Method mod. NIOSH 5040; TOA Approved by : JGC OSHA PEL NA Date : 31 -DEC -13 NYS DOH # : 11626 Collection Media 37mm QtzFt QC by: Tony D'Amico < -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms > -Greater Than ug -Micrograms 1 -Liters NS -Not Specified NA -Not Applicable ND -Not Detected ppm -Parts per Million Page 2 of 8 Report Reference:1 Generated:31-DEC-13 16:04 • GALSON LABORATORIES 6601 Kirkville Road East Syracuse, NY 13057 (315) 432-5227 FAX: (315) 437-0571 www.galsonlabs.com Client Site Project No. Date Sampled Date Received Date Analyzed Report ID LABORATORY ANALYSIS REPORT Indoor Environment Group Scandia 4055-002 17 -DEC -13 Account No.: 23406 20 -DEC -13 Login No. L307847 27 -DEC -13 813160 Diesel Particulate Matter as Carbon Air Vol Total Conc Sample ID Lab ID liter Analyte ug ug/m3 DP5-01 L307847-10 847.4 Organic Carbon 13 15 Elemental Carbon <3 <3 Total Carbon 13 15 COMMENTS: Please see attached lab footnote report for any applicable footnotes. Level of quantitation: 3ug OC & EC; 5ug TC Analytical Method mod. NIOSH 5040; TOA OSHA PEL NA Collection Media 37mm QtzFt Submitted by: JAR Approved by : JGC Date : 31 -DEC -13 NYS DOH # : 11626 QC by: Tony D'Amico -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms > -Greater Than ug -Micrograms 1 -Liters NS -Not Specified NA -Not Applicable ND -Not Detected ppm -Parts per Million Page 3 of 8 Report Reference:1 Generated:31-DEC-13 16:04 • GALSON LABORATORIES 6601 Kirkville Road East Syracuse, NY 13057 (315) 432-5227 FAX: (315) 437-0571 www.galsonlabs.com Nitrogen Dioxide Client Site Project No. Date Sampled Date Received Date Analyzed Report ID LABORATORY ANALYSIS REPORT Indoor Environment Group Scandia 4055-002 17 -DEC -13 Account No.: 23406 20 -DEC -13 Login No. L307847 23 -DEC -13 812689 COMMENTS: Please see attached lab footnote report for any applicable footnotes. PPM <0.03 <0.03 <0.03 <0.03 Level of quantitation: 0.5 ug Submitted by: tmk Analytical Method In-house: IC -SOP -14; IC Approved by : dnf OSHA PEL 5 ppm CEIL Date : 31 -DEC -13 NYS DOH # : 11626 Collection Media 500-200 QC by: Tony D'Amico < -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms > -Greater Than ug -Micrograms 1 -Liters NS -Not Specified NA -Not Applicable ND -Not Detected ppm -Parts per Million Page 4 of 8 Report Reference:1 Generated:31 -DEC-1 3 16:04 Time Total Conc Sample ID Lab ID minutes ucr ma/m3 N01-01 L307847-11 444 <0.5 <0.06 NO2-01 L307847-12 437 <0.5 <0.06 N04-01 L307847-13 428 <0.5 <0.07 N05-01 L307847-14 427 <0.5 <0.07 COMMENTS: Please see attached lab footnote report for any applicable footnotes. PPM <0.03 <0.03 <0.03 <0.03 Level of quantitation: 0.5 ug Submitted by: tmk Analytical Method In-house: IC -SOP -14; IC Approved by : dnf OSHA PEL 5 ppm CEIL Date : 31 -DEC -13 NYS DOH # : 11626 Collection Media 500-200 QC by: Tony D'Amico < -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms > -Greater Than ug -Micrograms 1 -Liters NS -Not Specified NA -Not Applicable ND -Not Detected ppm -Parts per Million Page 4 of 8 Report Reference:1 Generated:31 -DEC-1 3 16:04 • GALSON LABORATORIES 6601 Kirkville Road East Syracuse, NY 13057 (315) 432-5227 FAX: (315) 437-0571 www.galsonlabs.com Client Site Project No. Date Sampled Date Received Date Analyzed Report ID LABORATORY ANALYSIS REPORT Indoor Environment Group Scandia 4055-002 17 -DEC -13 Account No.: 23406 20 -DEC -13 Login No. L307847 23 -DEC -13 - 27 -DEC -13 812461 Respirable Dust and Crystalline Silica: Quartz Dust P E L mg % m m3 m m3 <0.050 <0.047 5.0 <0.010 ND <0.0093 <0.050 <0.047 5.0 <0.010 ND <0.0094 <0.050 <0.048 5.0 <0.010 ND <0.0096 <0.050 <0.047 5.0 <0.010 ND <0.0095 <0.050 <0.048 5.0 <0.010 ND <0.0097 COMMENTS: Please see attached lab footnote report for any applicable footnotes. Level of quantitation: Dust 0.050mg Q:0.010mg Submitted by: MNS/AJD/LCC Analytical Method Air Vol Sample ID Lab ID Analyte 1 RD1-01 Collection Media L307847-1 PW Dust 1074.06 Quartz 1074.06 RD2-01 L307847-2 Dust 1061.91 Quartz 1061.91 RD3-01 L307847-3 Dust 1040.04 Quartz 1040.04 RD4-01 L307847-4 Dust 1054.62 Quartz 1054.62 RD5-01 L307847-5 Dust 1032.75 Quartz 1032.75 Dust P E L mg % m m3 m m3 <0.050 <0.047 5.0 <0.010 ND <0.0093 <0.050 <0.047 5.0 <0.010 ND <0.0094 <0.050 <0.048 5.0 <0.010 ND <0.0096 <0.050 <0.047 5.0 <0.010 ND <0.0095 <0.050 <0.048 5.0 <0.010 ND <0.0097 COMMENTS: Please see attached lab footnote report for any applicable footnotes. Level of quantitation: Dust 0.050mg Q:0.010mg Submitted by: MNS/AJD/LCC Analytical Method mod. NIOSH 0600/7500/mod. OSHA ID -142; Gr Approved by : KRK OSHA PEL see 1910.1000 (Table Z-3) Date : 30 -DEC -13 NYS DOH # : 11626 Collection Media PVC PW QC by: Tony D'Amico < -Less Than mg -Milligrams > -Greater Than ug -Micrograms NA -Not Applicable ND -Not Detected mppcf -Million Particles per Cubic Foot m3 -Cubic Meters kg -Kilograms 1 -Liters NS -Not Specified ppm -Parts per Million Page 5 of 8 Report Reference:1 Generated:31-DEC-13 16:04 • GALSON LABORATORIES 6601 Kirkville Road East Syracuse, NY 13057 (315) 432-5227 FAX: (315) 437-0571 www.galsonlabs.com LABORATORY FOOTNOTE REPORT Client Name Indoor Environment Group Site Scandia Project No. 4055-002 Date Sampled : 17 -DEC -13 Account No.: 2340.6 Date Received: 20 -DEC -13 Login No. : L307847 Date Analyzed: 23 -DEC -13 - 27 -DEC -13 Unless otherwise noted below, all quality control results associated with the samples were within established control limits or did not impact reported results. Unrounded results are carried through the calculations that yield the final result and the final result is rounded to the number of significant figures appropriate to the accuracy of the analytical method. Please note that results appearing in the columns preceeding the final result column may have been rounded in order to fitthe report format and therefore, if carried through the calculations, may not yield an identical final result to the one reported. The stated LOQs for each analyte represent the demonstrated LOQ concentrations prior to correction for desorption efficiency (if applicable). Unless otherwise noted below, reported results have not been blank corrected for any field blank or method blank. L307847 (Report ID: 813160): SOPS: ic-n5040(16) Accuracy and mean recovery data presented below is based on a 95% confidence interval (k=2). The estimated uncertainty applies to the media, technology, and SOP referenced in this report and does not account for the uncertainty associated with the sampling process. Parameter Accuracy Mean Recove Diesel Particulate Matter as Carbon +/-7.1% 102% L307847 (Report ID: 812689): SOPS: IC -SOP -14(6) Total ug corrected for a desorption efficiency of 102%. Accuracy and mean recovery data presented below is based on a 95% confidence interval (k=2). The estimated uncertainty applies. to the media, technology, and SOP referenced in this report and does not account for the uncertainty associated with the sampling process. Parameter Accuracy Mean Recovery Nitrogen Dioxide +/-16.7 100% L307847 (Report ID: 812461): Dust analytical accuracy is within +/- 0.010 mg (95% confidence interval or k=2). The estimated uncertainty applies to the media, technology, and SOP(s) referenced in this report and does not account for any uncertainty associated with the sampling process. SOPS: GRAV-SOP-5(5), GRAV-SOP-6(4), ix-calibrate(8), ix-xrdashprep(19), ix-xrdreview(9), ix-xrdstdprep(20) Accuracy and mean recovery data presented below is based on a 95% confidence interval (k=2). The estimated uncertainty applies to the media, technology, and SOP referenced in this report and does not account for the uncertainty associated with the sampling process. Parameter Accuracy Mean Recovery Quartz +/-13.4% 95.1% < -Less Than mg -Milligrams m3 -Cubic Meters kg -Kilograms > -Greater Than ug -Micrograms 1 -Liters NS -Not Specified NA -Not Applicable ND -Not Detected ppm -Parts per Million Page 6 of 8 Report Reference:1 Generated:31-DEC-13 16:04 n 12 W C: E *-4 L 0 u C: (D E cr a— 0 E '5 N V# �c U) Z Z '2 CD m < 2 0 cr 4- or- (D 0) 4-- ra L) > -0 Ln CD Z� - co 0 m cn 0 r4 :Ll 0 2 .2) ,� a- C13 w 0 %a CL 40� V4 a. 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